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The title compound, bis(1,2-diphenyl-2-sulfanylideneethanethiolato-κ 2 S , S ′)(1,3,5-triaza-7-phosphaadamantane-κ P )cobalt(II) dichloromethane hemisolvate, [Co(pdt) 2 (PTA)]·0.5C 2 H 4 Cl 2 or [Co(C 14 H 10 S 2 ) 2 (C 6 H 12 N 3 P)]·0.5C 2 H 4 Cl 2 , contains two phenyldithiolene (pdt) ligands and a 1,3,5-triaza-7-phosphaadamantane (PTA) ligand bound to cobalt with the solvent 1,2-dichloroethane molecule located on an inversion center. The cobalt core exhibits an approximately square-pyramidal geometry with partially reduced thienyl radical monoanionic ligands. The supramolecular network is consolidated by hydrogen-bonding interactions primarily with nitrogen, sulfur and chlorine atoms, as well as parallel displaced π-stacking of the aryl rings. The UV–vis, IR, and CV data are also consistent with monoanionic dithiolene ligands and an overall Co II oxidation state.more » « less
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Brannon, Jacob P. ; Ramirez, Isaac ; Williams, DaShawn ; Barding, Gregory A. ; Liu, Yan ; McCulloch, Kathryn M. ; Chandrasekaran, Perumalreddy ; Stieber, S. Chantal ( , Journal of Chemical Education)null (Ed.)
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Jayarathne, Upul ; Chandrasekaran, Perumalreddy ; Greene, Angelique F. ; Mague, Joel T. ; DeBeer, Serena ; Lancaster, Kyle M. ; Sproules, Stephen ; Donahue, James P. ( , Inorganic Chemistry)